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Norwegian University of Life Sciences
1432 Ås
Norway

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Universitetet for miljø- og biovitenskap (UMB)

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Info http://athene.umb.no/emner/KJM240/
KJM240 Analytical Chemistry
Course responsible Elin Lovise Gjengedal IPM
   
Number of credits allocated 10.0
Language Norwegian
Limits for class size -
Semester/trimester
August block Autumn parallel January block Spring parallel June block
       
         
Colour explanation: Red/yellow = teaching periods. The red period indicates when the teaching starts.
Teachers Roland Kallenborn (IKBM; lecturer in chromatography), Karl Andreas Jensen, Solfrid Lohne.
Type of course Lectures: 4 hours per week (ca. 30 hours in all).
Laboratory exercises: 6 hours (1 day) per week (42 hours in all).
Compulsory educational activities Approved journal; 7 laboratory exercises.
Prerequisites KJM100 General Chemistry
Recommended prerequisites KJM120 Inorganic Chemistry, KJM230 Physical Chemistry.
Exam S
Assessment methods Final written examination (3.5 hours).
Grading A-F
Examination aids B1: distributed calculator, no other aids.
Nominal workload Lectures: 30 hours, laboratory exercises: 42 hours, completing 7 reports: 122 hours, self-tuition: 116 hours, a total workload of 300 hours.
Course frequency Annually
Comment on frequency -
Teaching methods Analytical chemistry is an experience-based subject where especially laboratory exercises are central.
Lectures are to give a broad introduction to analytical chemistry from sampling to the performing of analyses.
The laboratory exercises place emphasis on the critical evaluation of sources of error and uncertainty in the analyses that affect the interpretation of the data.
The laboratory reports are written as articles. The deadline for submitting a laboratory report is one week after the exercise has been conducted.
Teaching support The laboratory exercises place emphasis on the critical evaluation of sources of error and uncertainty in the analyses that affect the interpretation of the data. The students are free to make appointments for discussions with both the lecturer and the technical staff. The laboratory reports are written as articles. The deadline for submitting a laboratory report is one week. Each student will be given an opportunity to discuss improvements of the reports, even reports that are approved.
Examiner The examiner will be involved in the planning, conduction and revision (evaluation) of the course. The final examination and a selection of journals counting towards the final grade will be assessed in the regular manner.
Entrance requirements Special requirements in Science
Preferential right M-KJEMI, B-KJEMI, M-MINA, B-MINA, M-LUN, M-KB, NATURAL SCIENCE.
   
Note  
The course begins the first week of the autumn parallel. Compulsory attendance on the first lecture.
Laboratory exercises take place class by class with groups of up to 16 students, maximum 32 students. Assignment of students to the cource is based on preference and is adminitrated by responsible lecturer.
   
Objective of course  

Mainly to acquire a broad overview of inorganic analytical chemistry from the taking of samples to analysis. Through laboratory exercises, students are to learn how to critically evaluate sources of error and uncertainty in the analyses that influence the interpretation of data. Knowledge of how to take samples of water, soil and vegetation, as well as sample preparation methods and separation techniques. Knowledge of quality control with special emphasis on the validation of methods. Knowledge and understanding of the principles for the following analysis methods: Gravimetry and titer analysis. Titrimetrical methods (neutralisation, felling, complex, electrochemical methods, redox titrations and potentiometric methods). Spectroscopic methods (molecular absorption spectroscopy as well as atom spectroscopy based on absorption and emission). Gas and liquid chromatographical methods. Be able to select the most appropriate sample-taking, preparation and analysis methods based on accuracy requirements and possibly on knowledge about the sample's composition and economical limits. Evaluate the quality of analysis data. The course focuses on naturally occurring processes in the biogeochemical cycle, and in that way satisfies the environmental profile of UMB.

   
Course contents  
Lectures: The textbook, which gives an overview of the course and the theoretical background for relevant methods, is used as the point of departure. The laboratory exercises focus on naturally occurring processes in the biogeochemical cycle. The exercises give an introduction to inorganic analytical chemistry from sampling to the performing of analyses through practical experience. The laboratory exercises comprise both traditional and modern analysis methods. Another goal for the laboratory exercises is to teach students to write their lab reports as scientific articles.
   
Syllabus  
Textbook: Harris D.C. 2010 Quantitative Chemical Analysis. 8th Ed. W. H. Freeman and Company, N.Y.
 
Last updated 2012-03-23